Hockmeyer has introduced its new high viscosity immersion mills. The new HCPS series is capable of milling viscosities as high as 1,000,000 cps. They can be equipped with two different types of sweep blades: the Sidewall Scraper for thixotropic materials, and the Anchor Helix Scraper blade for heavier, tackier materials.
The HCPS is also fitted with an auger extending out of its upper draft tube, enabling the mill to pull material above the upper draft tube and feed it into the media field below for grinding.
The Sidewall Scraper
The Sidewall Scraper consists of a single rod connected to a concentric hub that rotates around the mill assembly. Teflon scrapers are stacked on top of each other in a continuous row, thus allowing coverage of the entire sidewall of the tank. The concentric hub can rotate clockwise or counterclockwise to suit the needs of the product.
As the scraper rotates clockwise, it creates a flow away from the sidewall of the tank and into the auger, thus allowing the operator to feed heavier material into the auger zone. When reversed, the Sidewall Scraper breaks the vortex of lower viscosity material, acting as a baffle.
The new design uses the batch itself to press the scrapers against the sidewall, eliminating the need for springs used in more conventional type scrapers. The purpose is to aid in flow control for lower viscosity, highly thixotropic materials. That, combined with our flow-thru scraper support, makes them easier to clean (no nuts or bolts), easier to change (no tools required), and more efficient for milling (self purging). The bottom of the jacketed tank is kept film-free by the turbulence created from the bottom propeller of the mill when this type of shear thinning material is milled. The turbulent flow from the bottom propeller also promotes substantial heat transfer.
Cooling with the Sidewall Scraper: Three Heat Transfer Conditions
1. Conduction – The transfer of heat through a fixed material like a tank wall into the cooling water jacket.
2. Convection – The transfer of heat between relatively hot portions and cool portions of the same liquid.
3. Radiation – The transfer of heat from a liquid surface to a gas above the surface.
The Anchor Helix Scraper
The Anchor Helix Scraper is a helical design with only one riser and a bottom leg. The tank is scraped both on its sidewall and across the bottom.The Anchor Helix Scraper is designed for products that are higher in density and viscosity than intended for the Sidewall Scraper. Such products would likely not blast off the tank bottom from the mill discharge or rise to the top for turnover without supplementary agitation. The Anchor Helix Scraper provides this agitation, preventing hot spots and stratification.
The Anchor Helix Scraper is designed to scrape in the counterclockwise direction only. As the tank walls are being scraped, milled product from the bottom of the tank rides along the helical riser toward the top of the tank where it is pulled back into the mill by the auger.
Cooling with the Anchor Helix Scraper
The Anchor Helix Scraper is an excellent cooling device for slow flowing products high in density. It is more effective in heat transfer than the Sidewall Scraper under these conditions.
The Sidewall Scraper creates a forced conduction zone and a forced convection zone while both it and the mill are in operation.The Anchor Helix Scraper can create these zones without the mill in operation. It becomes even more effective when the third type of heat transfer, forced radiation, is considered because of the uniform top to bottom turnover of the batch provided by the helix.
Although forced radiation is the least effective for cooling, it nonetheless adds to improve the overall heat transfer. The combination of all three types of heat transfer and the additional scraping of the cooling surface area at the bottom of the tank give the Anchor Helix Scraper significant advantage over the Sidewall Scraper on high density products that are not free flowing.
When to Use Which Scraper
The Sidewall Scraper is most efficient when used on lower density, thixotropic, free flowing materials. The Anchor Helix Scraper is most efficient when used on higher density products that are slow flowing, not necessarily thixotropic and will not turn over without supplementary agitation.
The HCPS has an auger in the mill’s upper draft tube enabling it to grab material from above the mill chamber and force it into the media field. Without the auger, the efficiency of the mill would be greatly reduced. The auger has multiple effects on the Immersion Mill:
• Feeds highly viscous material into the grind chamber.
• Acts as a governor to control feed rate into the grind chamber.
• Acts as a seal to prevent floating or “burping” of media as mill is immersed.
• Entrapped air exits the bead field through the screens instead of the upper draft tube.
• Prevents film formation inside upper draft tube, enhancing cooling.
The upper draft tube is fitted with a wear resistant, high heat transfer sleeve that prevents abrasive material from wearing into the cooling chamber surrounding it. The auger is split on larger models to permit easy removal access for cleaning.
The upper draft tube of the HCPS is cooled. Without the auger, a film may form inside the upper draft tube while the mill is running, making the effect of cooling in the tube limited. With the addition of the auger a film does not form. Cool material is constantly scraped off and augured into the media field as it is replaced with incoming material creating both additional Forced Conduction and Force Convection Zones.
Engaging the Problems of Scale-Up Cooling
Scaling up from lab size machines to production size machines requires special measures to keep the batch cool. The available cooling surface area of a production tank is much smaller per gallon of product than that of a laboratory tank.
For example: One gallon in a 7” diameter x 6” tall tank, jacketed on the side and bottom, has a cooling surface of 170 square inches per gallon. One hundred gallons in a 31” diameter x 31” tall tank jacketed on the side and bottom has a cooling surface of 38 square inches per gallon, a very substantial reduction of 132 square inches per gallon.
The way to best control heat is by developing a forced conduction zone, a forced convection zone and a forced radiation zone in the tank simultaneously. This is accomplished by physically scraping cool material from the tank walls, mixing the cool material with the hot material and exposing the hot material to a cooler atmosphere above the batch. A nitrogen purge can be used to further the radiation cooling. The use of internal tank cooling baffles or coils would interfere with flow during high viscosity milling and counterproductive. Accordingly, they are not taken into consideration.
While it is true that the lost surface area per gallon cannot, under the circumstances, be regained, it can be made substantially more efficient through the use of scraped surface agitation.
Other variables to consider in heat transfer include:
1) Conductivity of the material being milled: If the batch has poor or non-conductive ingredients, temperature can build quickly and become difficult to remove.
2) Viscosity: As it rises, if equipment and cooling variables remain constant, batch temperature will rise.
3) Shear: Tends to increase temperature as viscosity increases.
4) Solids Content: Increasing solids content tends to increase shear and temperature.
5) Cooling water temperature: Must be adjustable to help insure predictable temperature control.
The addition of the Anchor Helix Scraper or the Sidewall Scraper and the auger has greatly increased the ability of the Immersion Mill to effectively operate in viscosity ranges that were previously beyond its capabilities.
The new HCPS High Viscosity Immersion Mills will allow companies to shift many products away from the roller mills. Not all roller mill formulations are capable of being run on the HCPS, but many can be if the formulas are adjustable enough to permit a forced flow during the milling process. If they can be mixed by the helix, they can be milled by the HCPS.
Many formulas produced on roller mills are adjusted with letdown after the milling process has been completed. This is sometimes done intentionally because roller mills work best when viscosities, densities and tack are high. The elimination of let down after milling enhances the efficiency of the HCPS, making it a one-step process.
The new “HCPS” series Immersion Mills require minimal operator interface, unlike roller mills that require frequent monitoring. They can be equipped with APC-II (Auto Process Control) systems that control water flow, slowdown temperature, shutdown temperature, alarm temperature and batch run time. These adjustable parameters make the HCPS Immersion Mills labor saving, batch monitors.